Preparation Of Ammonium IodidePreparation Of Ammonium Iodide

254 g of potassium iodide dissolved in 125 ml of water are mixed with 100 g of ammonium sulfate dissolved in 125 ml of boiling water.

After cooling, 40 ml of alcohol are added and the mixture is kept 12 hours. The obtained precipitate of potassium sulfate is filtered and the filtrate is evaporated occasionally adding ammonia water containing some alcohol, until crystallization begins.

The crystals of potassium sulfate are additionally washed with dilute alcohol (20%), and after combining the filtrates and evaporation the ammonium iodide is obtained. Ammonium iodide crystallizes in cubes and deliquesces in the air. It should be preserved in a dark place, as light decomposes the salt, causing it to turn brown. This coloration may be removed by dissolving in distilled water, treating the solution with ammonium sulfide, filtering, and evaporating the filtrate on the steam bath, to crystallize. It is readily soluble in alcohol.

The aqueous solution becomes yellow on standing, owing to decomposition and separation of iodine.

One part of the salt dissolves in 0.60 part of water.

Nanjing Chemical Material Corporation. (NCMC), is a professional chemical distributor company, we provide DMC catalyst, monoammonium glycyrrhizinate, methyl Iodide, allyl glycidyl ether, glycolic acid and etc. Want to know more? Please contact us.

Comments

Difference Between Sulfate And Sulfonate In Shampoo

Sulfates and sulfonates have two things in common. First, they're all anionic surfactants. Second, they are often used for personal care applications. But there are many differences. They have different molecular mechanisms. They have different functions and they have different raw materials. Sulfates Sulfate is a compound. It has carbon bonds and oxygen and sulfur bonds. They include substances such as sodium lauryl sulfate and sodium lauryl ether sulfate. At low pH, these substances plus the c-o-s bond hydrolyze to produce alcohol and inorganic sulfate. At a high pH, sulfate is stable in the base and, if ethoxylated to a relatively high level, produces a low-foaming alkali-soluble surfactant. Sulphates can be prepared by reaction of fatty alcohol or fatty alcohol ethoxylates with reagents such as SO3 or chlorosulfonic acid (CSA). The reason shampoo becomes thick foam in the shower is that it contains sulfate. Most shampoos and household cleansers contain su...

Two Different Types of Anionic Surfactants

Anionic surfactant is a kind of product with the longest history, the largest output and the most varieties among surfactants. According to the structure of hydrophilic groups, anionic surfactants can be divided into sulfonates and sulfates, which are the main categories of anionic surfactants. The anionic surfactants definition is a must-known concept for many people working in the chemical industry. The various functions of surfactants are mainly manifested in changing the properties of the liquid surface, liquid-liquid interface and liquid-solid interface, of which the surface (interface) of the liquid is the most important. Sulfate-type anionic surfactants mainly include fatty alcohol sulfate (also known as primary alkyl sulfate) and secondary alkyl sulfate ： 1. Fatty alcohol sulfate (ester) salt (FAS or AS). The general formula of fatty alcohol sulfate is: ROS0-3M+, R is alkyl, M+ is sodium, potassium, ammonium, ethanolamine and other ca...

Polyether Polyol Manufacturing Process

Synthesis of DMC-based polyether polyol by a continuous method A certain amount of DMC catalyst is taken and uniformly dispersed in a certain amount of small molecule initiator. Add 0.5 kg of the mixture of the initiator in the small test reactor. The vacuum was replaced 1-2 times with N2, and the N2 pressure was maintained at 0.1 MPa. After heating, stirring and raising the temperature to a certain temperature, the quantitative PO was introduced into the continuous autoclave with nitrogen gas for induction. When the induction is successful (the temperature in the kettle rises and the pressure drops), the PO is continuously passed to carry out the reaction. Open the outer loop and continue to pass the PO into the continuous kettle. When the liquid in the reaction vessel is full, the PO, DMC catalyst and the initiator are continuously added to the kettle at a certain ratio and a certain speed through the power system. Continuous discharge is started when a certain pr...

Nanjing Chemical Material Corp.

Search This Blog